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Page 1 od 77 rezultati
Cyclodextrin cavity size effect on the complexation and rotational dynamics of the laser dye 2,5-diphenyl-1,3,4-oxadiazole: from singly occupied complexes to their nanotubular self-assemblies.
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The general complexation scheme as well as the dynamic features of the supramolecular structures resulting from the interaction of the laser dye 2,5-diphenyl-1,3,4-oxadiazole (PPD) with the naturally occurring alpha-, beta-, and gamma-cyclodextrins in water are studied by means of fluorescence
Molecular modulation of muscarinic antagonists. Synthesis and affinity profile of 2,2-diphenyl-2-ethylthio-acetic acid esters designed to probe the binding site cavity.
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The synthesis and preliminary pharmacological profile of a new series of muscarinic antagonists, derived from previously studied 2,2-diphenyl-2-ethylthio-acetic acid esters, are reported. The parent molecules were decorated with linkers of different length, carrying an amino group to catch a
Development of multi-frequency ESR/EDMR system using a rectangular cavity equipped with waveguide window.
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A straightforward method for a variable frequency electron spin resonance/electrically detected magnetic resonance (ESR/EDMR) spectroscopy using a C-band microwave cavity equipped with waveguide windows is presented. The method enables us to perform quasi-continuous multiple resonance frequency
Headspace solid-phase microextraction with novel sol-gel permethylated-beta-cyclodextrin/hydroxyl-termination silicone oil fiber for determination of polybrominated diphenyl ethers by gas chromatography-mass spectrometry in soil.
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A simple, sensitive, and accurate method for determination of polybrominated diphenyl ethers (PBDEs) in soil has been developed based on headspace solid-phase microextraction (HS-SPME) followed by gas chromatography-mass spectrometry (GC-MS). Permethylated-beta-cyclodextrin/hydroxyl-termination
Efficient fluorescent sensors based on 2,5-diphenyl[1,3,4]oxadiazole: a case of specific response to Zn(II) at physiological pH.
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The coordination properties and photochemical responses of three fluorescent polyamine macrocycles, 9,12,15,24,25-pentaaza-26-oxatetracyclo[21.2.1.0(2,7).0(17,22)]hexaicosa-2,4,6,17,19,21,23,25(1)-octaene (L1),
Exploring the binding features of polybrominated diphenyl ethers as estrogen receptor antagonists: docking studies.
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The polybrominated diphenyl ethers (PBDEs) accumulating in nature are known to be endocrine-disrupting compounds. Of first concern are those interacting with and altering activity of the human estrogen receptor alpha (hERalpha). In this study a docking study was carried out to explore the binding
Quantitative structure-activity relationship of 4,5-diphenyl-2-(substituted thio)-1H-imidazoles as the inhibitors of acyl CoA: cholesterol acyltransferase.
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A quantitative structure-activity relationship (QSAR) analysis of 4,5-diphenyl-2-(substituted thio)-1H-imidazoles as the potential inhibitors of acyl CoA: cholesterol acyltransferase is presented with a view to reflect upon the parametric requirement of various substitutions. For this purpose the
[UV spectroscopic characterization of the inclusion interaction of beta-cyclodextrin and sym-diphenyl-thiourea and sym-diphenyl-urea].
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The inclusion interaction of beta-cyclodextrin and sym-diphenyl-thiourea and sym-diphenyl-urea was studied by UV spectra. The stoichiometry ratio for the formation of the inclusion complexes was determined by Hildebrand-Benesi equation linear analysis and molar ratio method. The standard molar Gibbs
[Fluoride tolerance in cases of dental caries and fluorosis].
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32 volunteers (18-20-year-olds) without concomitant diseases were divided into 3 groups: with high caries incidence (1), with dental fluorosis of different degrees (2) and with completely intact dentition (3). Dynamics of ionized F in blood serum and mixed saliva after single sodium fluoride burden
Metalation and Selective Oxidation of Diphenyl-23-oxa-, -thia-, and -selena-21-carbaporphyrins.
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The availability of diphenyl-23-oxa-, -thia-, and -selena-21-carbaporphyrins has enabled the reactivity of these systems to be investigated and contrasted. All three heterocarbaporphyrins reacted with palladium(II) acetate in refluxing chloroform-acetonitrile to give organometallic palladium(II)
Chemiluminescence response of beta-glucan stimulated leukocytes isolated from different tissues and peritoneal cavity of Dicentrarchus labrax.
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The respiratory burst of leukocytes isolated from sea bass (Dicentrarchus labrax) pronephros, peritoneal cavity (P.C.), spleen and blood, was measured by a chemiluminescence (CL) assay after stimulation with beta-glucan. The CL response by P.C. and pronephros leukocytes was significantly higher than
Diphenyl diselenide reduces inflammation in the mouse model of pleurisy induced by carrageenan: reduction of pro-inflammatory markers and reactive species levels.
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OBJECTIVE
We reported the anti-inflammatory action of diphenyl diselenide [(PhSe)(2)] in an acute inflammation model induced by carrageenan.
METHODS
Male adult Swiss mice.
METHODS
Mice were treated with (PhSe)(2) (50 mg/kg) or vehicle (10 ml/kg) per oral route. After 30 min, animals received saline
LncRNA SNHG4 promotes the increased growth of endometrial tissue outside the uterine cavity via regulating c-Met mediated by miR-148a-3p
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Long noncoding RNAs (lncRNAs) modulate endometriosis. The current study investigated the mechanisms and effects of SNHG4 on endometriosis. The qRT-PCR was conducted to examine the miR-148a-3p and SNHG4 expressions in endometriosis tissues. The 5-ethynyl-2'-deoxyuridine incorporation assay and 3-(4,
Influence of the toothpaste with brazilian ethanol extract propolis on the oral cavity health.
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Propolis-based therapeutic agents represent this potential for the development of new drugs in dental care. The aim of a clinical-cohort study was to determine the influence of application of toothpaste enriched with Brazilian extract of propolis (EEP) on health status of oral cavity. Laboratory
Broadband electron spin resonance at low frequency without resonant cavity.
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We have developed a nonconventional broadband electron spin resonance (ESR) spectrometer operating continuously in the frequency range from 0.5 to 9 GHz. Dual antenna structure and the microwave absorbing environment differentiate the setup from the conventional one and enable broadband operation
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