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Cytotoxic Cardiac Glycoside Constituents of Vallaris glabra Leaves.
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Thirteen cardenolide glycosides (1-13) were isolated from the CH2Cl2 and MeOH extracts of Vallaris glabra leaves. The structures of the new compounds (2-13) were identified by spectroscopic methods, with the absolute configurations of the sugar moieties determined by acid hydrolysis. All compounds
Cytotoxic 20,22-Dihydrodigitoxigenin Glycosides and Other Constituents of Vallaris glabra Stems.
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Ten cardiac glycosides (1-10) including six 20,22-dihydrodigitoxigenin and four gitoxigenin glycosides were isolated from the stems of Vallaris glabra together with six known triterpenoid cinnamates. Spectroscopic data of these previously undescribed compounds are reported. All
[THE GLYCOSIDES OF THE SEEDS OF VALLARIS SOLANACEA (ROTH) O. K. ISOLATION. GLYCOSIDES AND AGLYCONES, 263].
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[THE GLYCOSIDES OF THE SEEDS OF VALLARIS SOLANACEA (ROTH) O.K. CLARIFICATION OF STRUCTURE. GLYCOSIDES AND AGLYCONES, 264].
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Acoschimperoside P, 2'-acetate: a Hedgehog signaling inhibitory constituent from Vallaris glabra.
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Complete (1)H and (13)C NMR assignments of acoschimperoside P, 2'-acetate (1) and a new cardiac glycoside (2), isolated from the leaves of Vallaris glabra, are described. Compound 1 was active in the assay for Hedgehog signaling inhibition. In further experiments, this compound showed a strong
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