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bakkenolide/ligularia
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[Terpenoid compounds isolated from Ligularia sagitta].
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OBJECTIVE
To study the chemical constituents of radix and rhizome of Ligularia sagitta.
METHODS
Isolation and purification were carried out on the column chromatography of silica gel and sephadex LH -20. The structures were identified by spectral analysis.
RESULTS
Seven terpenoid compounds were
Two new compounds from Ligularia dolichobotrys.
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Two new compounds, a stigmasterol (1) and an eremophilenolide (2), were isolated from Ligularia dolichobotrys (Diels) together with ten known sesquiterpenoids, two known triterpenes and five known sterols. Their structures were elucidated by spectroscopic methods (IR, MS, 1H, 13C and 2D NMR). In
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